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Pakawadee Sutthivaiyakit. Simultaneous determination of p-coumaric acid and naringenin in honey using dispersive liquid-liquid microextraction and high performance liquid chromatography. (). King Mongkut's University of Technology North Bangkok. Central Library. : , 2018.
Simultaneous determination of p-coumaric acid and naringenin in honey using dispersive liquid-liquid microextraction and high performance liquid chromatography
Name: Korbkarn Khukitirat
Organization :
Kasetsart University. Faculty of Science
Name: Pongsak Lowmunkhong
Organization :
Kasetsart University. Faculty of Science
Name: Somyote Sutthivaiyakit
Organization :
Ramkhamhaeng University. Faculty of Science
Name: Pakawadee Sutthivaiyakit
Organization :
Kasetsart University. Faculty of Science
Email :
fscipws@ku.ac.th
Abstract:
p-Coumaric acid and naringenin have anti-inflammatory and antioxidant benefits.
However, they have not been determined in honey from Thailand. A simple, rapid and
sensitive dispersive liquid-liquid microextraction (DLLME) followed by HPLC with diode
array detection was developed for simultaneous determination of the two compounds. Some
important parameters for DLLME were optimized. A mixture of acetonitrile disperser
solvent) and dichloromethane (extraction solvent) was rapidly injected to a sample solution in
0.01 M ammonium acetate adjusted to pH 3 by a syringe, thereby forming a cloudy solution.
After centrifugation at 4 °C, the enriched analytes in the sedimented phase were filtered prior
to injection. The separation was performed on a Pursuit XRS Diphenyl column (150x3.0
mm, 3 um) at 40 °C with 0.1% formic acid methanol gradient as the mobile phase. The
detection wavelengths were 291 nm and 311 nm for naringenin and p-coumaric acid,
respectively. The flow rate was 0.3 mL min-1. Due to the lack of matrix blank, standard
addition was performed in the method development. The concentrations of p-coumaric acid
and naringenin in lychee are 0.5±0.01ug.g-1 and 0.38 ± 0.03ug.g-1, respectively..
King Mongkut's University of Technology North Bangkok. Central Library
Address:
BANGKOK
Email:
library@kmutnb.ac.th
Created:
2018
Modified:
2562-06-27
Issued:
2019-06-27
บทความ/Article
application/pdf
BibliograpyCitation :
In Prince of Songkla University Faculty of Science. Pure and Applied Chemistry International Conference (PACCON 2018) (p.AN170-AN174). Songkla : Prince of Songkla University
eng
©copyrights King Mongkut's University of Technology North Bangkok
RightsAccess:
ใช้เวลา
0.034672 วินาที
Korbkarn Khukitirat
| Title | Contributor | Type |
|---|---|---|
| Simultaneous determination of p-coumaric acid and naringenin in honey using dispersive liquid-liquid microextraction and high performance liquid chromatography
มหาวิทยาลัยเทคโนโลยีพระจอมเกล้าพระนครเหนือ Korbkarn Khukitirat;Pongsak Lowmunkhong;Somyote Sutthivaiyakit;Pakawadee Sutthivaiyakit | บทความ/Article |
Pongsak Lowmunkhong
| Title | Contributor | Type |
|---|---|---|
| Studies of corrosion inhibitors for mild steel by delectrochemical techniques
มหาวิทยาลัยเกษตรศาสตร์ Pongsak Lowmunkhong | Pakawadee Sutthivaiyakit | วิทยานิพนธ์/Thesis |
| Paper-based ammonia gas sensor using zinc complex of Eriochrome Black T and digital image analysis
มหาวิทยาลัยเทคโนโลยีพระจอมเกล้าพระนครเหนือ Supa Sangdang;Pongsak Lowmunkhong;Pakawadee Sutthivaiyakit | บทความ/Article | |
| Simultaneous determination of p-coumaric acid and naringenin in honey using dispersive liquid-liquid microextraction and high performance liquid chromatography
มหาวิทยาลัยเทคโนโลยีพระจอมเกล้าพระนครเหนือ Korbkarn Khukitirat;Pongsak Lowmunkhong;Somyote Sutthivaiyakit;Pakawadee Sutthivaiyakit | บทความ/Article | |
| Method development for determinatioin of chloramphenicol and semicarbazide in food samples
มหาวิทยาลัยเกษตรศาสตร์ Pongsak Lowmunkhong | Pakawadee Sutthivaiyakit | วิทยานิพนธ์/Thesis |
Somyote Sutthivaiyakit
| Title | Contributor | Type |
|---|---|---|
| Simultaneous determination of p-coumaric acid and naringenin in honey using dispersive liquid-liquid microextraction and high performance liquid chromatography
มหาวิทยาลัยเทคโนโลยีพระจอมเกล้าพระนครเหนือ Korbkarn Khukitirat;Pongsak Lowmunkhong;Somyote Sutthivaiyakit;Pakawadee Sutthivaiyakit | บทความ/Article |
Pakawadee Sutthivaiyakit
| Title | Contributor | Type |
|---|---|---|
| Paper-based ammonia gas sensor using zinc complex of Eriochrome Black T and digital image analysis
มหาวิทยาลัยเทคโนโลยีพระจอมเกล้าพระนครเหนือ Supa Sangdang;Pongsak Lowmunkhong;Pakawadee Sutthivaiyakit | บทความ/Article | |
| Simultaneous determination of p-coumaric acid and naringenin in honey using dispersive liquid-liquid microextraction and high performance liquid chromatography
มหาวิทยาลัยเทคโนโลยีพระจอมเกล้าพระนครเหนือ Korbkarn Khukitirat;Pongsak Lowmunkhong;Somyote Sutthivaiyakit;Pakawadee Sutthivaiyakit | บทความ/Article |