Tinnakorn Tiensing. Method development for the determination of alkanolamines using high performance liquid chromatography. (). King Mongkut's University of Technology North Bangkok. Central Library. : , 2017.
Method development for the determination of alkanolamines using high performance liquid chromatography
Abstract:
Triethanolamine (TEA) and triisopropanolamine (TiPA) are both of the
alkanolamines used in many industrial applications. The determination of these compounds in
industrial product plays an important role in quality control for the production process. This
research was developed a reliable method for the determination of TEA and TiPA using high
performance liquid chromatography (HPLC). The studied compounds of TEA and TiPA were
separated on a C18 column, EC250/4.6 NUCLEODUR 100-5 using a mobile phase of 2 mM
sodium acetate solution and acetonitrile at the ratio of 80:20 (v/v). The UV-Vis detector was
set at wavelength of 210 nm. Linear range was successfully performed in the study range
(TEA: 1-100 ppm, TiPA: 3-100 ppm) with good linear correlation. Limit of detection (LOD)
were 0.3 and 0.9 ppm for TEA and TiPA, respectively. Also, the quantitation limit of the
HPLC system was 1.1 ppm for TEA and 3.0 ppm for TiPA analysis.
King Mongkut's University of Technology North Bangkok. Central Library
Address:
BANGKOK
Email:
library@kmutnb.ac.th
Created:
2017
Modified:
2562-07-23
Issued:
2019-07-23
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BibliograpyCitation :
In Chemical Society of Thailand under the Patronage of Her Royal Hghness Princess Chulabhorn Mahidol and King Mongkut's University of Technology North Bangkok Faculty of Applied Science. Pure and Applied Chemistry International Conference (PACCON 2017) (pp.108-112). Bangkok : Chemical Society of Thailand under the Patronage of Her Royal Hghness Princess Chulabhorn Mahidol